An innovative green electrode architecture employing ON–OFF fluorescence signaling proposed to enhance the adsorption and controlled release of Ag and Pb ions to improve the reaction efficiency and minimize metal loss in the electro-click triazole named reaction

Key Points

• The aim is to enhance the reaction efficiency in triazole synthesis by improving metal ion management and minimizing loss.
• Developed a GO-supported ATPB@Ag/Pb electrocatalyst
• Employed ON–OFF fluorescence signaling for monitoring
• Implemented pH-controlled release and recovery of metals
• Assessed reusability across 12 cycles
• Demonstrated effective fluorescence signaling for metal management
• Achieved high reusability with minimal leaching of metals
• Enhanced efficiency in the synthesis of triazoles