Crystal structure of bis(mesityl)-bis( μ 2 -(2-(dimethylamino)phenyl)((2-(dimethylamino)phenyl) carbamoyl)amidato)-bis( μ 2 -carbonylbis((2-(dimethylamino)phenyl)amidato) )tetrairon(II) toluene solvate

Key Points

• To determine the crystal structure of a tetrairon(II) complex with amidato ligands.
• Monoclinic crystal structure analysis of C100H120Fe4N16O4 using X-ray crystallography at 103 K.
• Measurements included unit cell parameters: a = 31.7817 Å, b = 13.1715 Å, c = 22.4686 Å, β = 100.407°.
• Refinement metrics: Rgt(F) = 0.0906, wRref(F2) = 0.0961.
• The structure was confirmed to be monoclinic with a volume of 9250.9 ų.
• The complex exhibits a unique arrangement of bis(mesityl) and amidato ligands.
• All structural parameters were accurately measured, contributing to the understanding of tetrairon complexes.