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March 3, 20260 citationsOpen Access

Comparative Effect of Different Nanoparticles with Different Concentrations on Fracture Toughness and Elastic Modulus of Restorative Dental Composite Resin

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MHMohamed Ahmed HelalEAEmad Amin AzmyAAAmal Al-Faraj

Key Points

  • This research aims to evaluate how different nanoparticles and their concentrations affect the mechanical properties of a dental composite resin.
  • Constructed 140 rectangular specimens for testing based on ISO standards.
  • Specimens categorized into control and three modified groups with different nanoparticles (ZrO2, TiO2, SiO2).
  • Performed fracture toughness testing using single-edge notched beams and elastic modulus testing using three-point bending.
  • Conducted data analysis with two-way ANOVA and Bonferroni post hoc tests.
  • ZrO2 improved both elastic modulus (E) and fracture toughness (KIC) the most, especially at 3 wt% for stiffness and 7 wt% for toughness.
  • TiO2 enhanced mechanical properties, but less effectively than ZrO2.
  • SiO2 improved performance at 3 wt%, but decreased values at 7 wt%.

Abstract

Background/Objective: Resin-based composite (RBC) gained wide popularity in dentistry due to its excellent biocompatibility, superior aesthetics, and good bonding to enamel and dentine. However, they have several shortcomings, including mechanical insufficiency and shrinkage tendency. Many researchers have utilized nanoparticles (NPs) as a reinforcing filler for RBCs. This article focused on assessing the impact of three different nanoparticles, ZrO2, TiO2, and SiO2, with concentrations of 3 wt% and 7 wt%, on the elastic modulus (E) and fracture toughness (KIC) of one commercial light-activated dental resin composite. Methods: 140 rectangular specimens were constructed according to ISO 4049 with dimensions (25 × 2 × 5 ± 0.03 mm) and (25 × 2 × 2 ± 0.03 mm) for fracture toughness and elastic modulus, respectively. Specimens were categorized into four main groups based on nanofiller types. Control: plain without filler (CC) and three modified ones with ZrO2 (ZC), TiO2 (TC), and SiO2 (SC). Furthermore, modified groups were divided into two subgroups according to nanofiller concentration, 3 and 7 wt% (ZC3, ZC7, TC3, TC7, SC3, and SC7), n = 10. Mechanical testing for fracture toughness was completed using a single-edge notched beam, while a three-point bending test was used for elastic modulus. Analysis of data was based on two-way ANOVA and Bonferroni post hoc (α = 0.05). Results: ZrO2 provided the most substantial improvement in both E and KIC, with the optimal performance observed at 3 wt% for stiffness and 7 wt% for toughness. TiO2 groups also enhanced these properties at both concentrations; however, the gains were less pronounced compared to ZrO2. SiO2 improved mechanical performance at 3 wt%, but a higher loading of 7 wt% resulted in reduced values. Conclusions: Resin-based composite modified with 3 wt% of NPs tends to possess higher fracture toughness and modulus of elasticity. Fracture toughness enhancement was concentration-dependent with ZrO2 NPs, where the best result was obtained with 7 wt%. Nanoparticle-reinforced composite, particularly ZrO2, may be suitable for prosthodontic applications.

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Cite This Study

Helal et al. (2026) studied this question.

synapsesocial.com/papers/69a67f12f353c071a6f0aeb3https://doi.org/10.3390/dj14030134
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