This work presents a scalable approach for synthesizing MXene/metal composites via direct etching of MAX phase/metal–Al alloy precursor materials. By combining Ti3AlC2 MAX phase with Ni–Al, Cu–Al, and Ni–Cu–Al alloys and optimizing sintering and etching conditions, the authors demonstrate the formation of three-dimensional porous MXene/metal architectures with enhanced electrochemical performance. The composites exhibit high activity toward the hydrogen evolution reaction and improved areal capacitance, highlighting their potential for energy conversion and storage applications.
Sergiienko et al. (Mon,) studied this question.
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