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March 4, 2026Journal of Analytical Atomic Spectrometry0 citationsOpen Access

Elemental analysis of air-sensitive frozen molten salt samples using an inert transfer chamber for LIBS/LA-ICP-TOF-MS analysis

PBPaul D. BennyPMPeggy T. MilotaSSSam Schultz

Key Points

  • This research aims to enhance the elemental analysis of air-sensitive molten salt samples post electrochemical experiments.
  • Developed an inert transfer system for transporting samples from glovebox to lab.
  • Utilized simultaneous LIBS and LA-ICP-TOF-MS techniques for analysis.
  • Performed analysis within a two-volume cell to maintain sample integrity.
  • Successfully transported air-sensitive frozen molten salt samples without contamination.
  • Demonstrated effective elemental analysis using the developed transfer system.
  • Resulted in accurate characterization of the molten salt compositions.

Abstract

A novel transfer system was used to transport air-sensitive frozen molten salt samples after electrochemical experiments from a glovebox to an analytical laboratory for simultaneous LIBS/LA-ICP-TOF-MS analysis in a two-volume cell.

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Cite This Study

Benny et al. (2026) studied this question.

synapsesocial.com/papers/69a7cdaed48f933b5eeda423https://doi.org/10.1039/d5ja00482a
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