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March 6, 2026SHILAP Revista de lepidopterología0 citationsOpen Access

Unveiling the physicochemical properties of CaMgBiNbO6 double perovskite oxide

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APAnita Kumari PandaRCRimpi ChakravartySSSantanu Sen

Key Points

  • The aim is to investigate the physicochemical properties of the CaMgBiNbO6 double perovskite oxide sample.
  • Utilized solid-state reaction method at 1150 °C for sample fabrication.
  • Conducted X-ray diffraction for crystallisation analysis.
  • Performed scanning electron microscopy for morphology assessment.
  • Measured dielectric and electrical properties over a wide temperature and frequency range.
  • Analyzed complex impedance and modulus parameters for relaxation phenomena.
  • Identified varied crystal symmetry phases during X-ray diffraction.
  • Observed an optimum UV absorption around 700 nm with a direct bandgap of approximately 2.75 eV.
  • Confirmed non-ideal relaxation behavior consistent with Koop's theory.
  • Derived characteristics of bulk/grain and grain barrier effects via Cole–Cole plot.
  • Indicated ferroelectric properties through P–E loop emergence.

Abstract

A solid-state reaction method involving high-temperature treatment at 1150 °C was employed to fabricate the CaMgBiNbO6 ceramic sample. X-ray diffraction analysis indicated the crystallisation of the specimen in various crystal symmetry phases and space groups. Scanning electron microscopy imaging revealed the polycrystalline morphology of the specimen. The UV absorption spectra exhibit an optimum wavelength of around 700 nm and a direct bandgap of approximately 2.75 eV. Dielectric and electrical measurements were conducted over the temperature range of 25–500 °C and a frequency sweep from 100 Hz to 5 MHz. The pattern observed in assessing the dielectric parameters of the sample is consistent with Koop’s theory and the Maxwell‒Wagner model. Analysis of the complex impedance and complex modulus parameters reveals that the sample undergoes a non-ideal relaxation phenomenon, unlike a Debye-like phenomenon. The role of bulk/grain and grain barrier effects on the impedance parameter is visualised by the Cole–Cole plot, and the NTCR nature is also verified. The emergence of the P–E loop suggests a ferroelectric property in the sample. These multifaceted properties of the studied CaMgBiNbO6 ceramic sample make it suitable for a variety of electronic applications.

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Cite This Study

Panda et al. (2026) studied this question.

synapsesocial.com/papers/69aa7048531e4c4a9ff59f34https://doi.org/10.1080/14786451.2026.2637276
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