The electrochemical behavior of tricyclic monoperoxide on a smooth gold electrode in an acetonitrile solution was studied by cyclic voltammetry (CV). It was found that the cathodic process involves the joint transfer of two electrons. In the anodic process, the electrode corrodes, forming gold nanoparticles. A mechanism for the reduction of monoperoxide to triketone was proposed.
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M. V. Polyakov
M. D. Vedenyapina
A. M. Skundin
Russian Journal of Physical Chemistry A
N.D. Zelinsky Institute of Organic Chemistry
Frumkin Institute of Physical Chemistry and Electrochemistry
D. Mendeleyev University of Chemical Technology of Russia
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Polyakov et al. (Thu,) studied this question.
www.synapsesocial.com/papers/69ada8a1bc08abd80d5bbc82 — DOI: https://doi.org/10.1134/s0036024425703133
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