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March 12, 2026Materials & Design1 citationsOpen Access

Sequential immunomodulation-osteogenesis by zinc-loaded nanotopographical fibrous membranes for inflammatory alveolar bone regeneration

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BZBowen ZhengJLJiacheng LvCGCui-Ting Gao

Key Points

  • The study aims to explore the effects of zinc-loaded membranes on immunomodulation and osteogenesis for alveolar bone regeneration in periodontitis.
  • Developed zinc-loaded polycaprolactone fibrous membranes via electrospinning and crystallization.
  • Examined macrophage polarization and bone marrow stem cell differentiation in vitro.
  • Assessed the regeneration of alveolar bone in vivo by evaluating immune microenvironments.
  • Zn 2+ leads to M2 macrophage polarization while inhibiting M1 polarization.
  • Enhanced osteogenic differentiation observed in bone marrow mesenchymal stem cells.
  • The membranes effectively remodel the immune microenvironment, boosting bone regeneration.

Abstract

• Developed a Zn 2+ -loaded nanotopographical PCL fibrous membrane via electrospinning and epitaxial crystallization. • The surface topography primarily inhibits M1 macrophage polarization, while Zn 2+ release promotes M2 polarization. • A synergistic immunomodulatory effect reshapes the osteoimmune microenvironment in periodontitis. • Sequential regulation of “immunomodulation first, osteogenesis second” enhances alveolar bone regeneration. • Provides a novel bioactive material strategy for treating inflammatory bone defects in periodontitis. The regeneration of alveolar bone defects resulting from periodontitis poses a significant challenge in dental medicine, as it involves coordinated regulation of multiple biological processes, including anti-inflammation, osteogenesis, and immunomodulation. While engineered fibrous scaffolds enabling sustained bioactive release and providing physical topographical cues have been developed, current materials still face limitations in effectively balancing immunomodulation with biocompatibility. Herein, we constructed a zinc-loaded nanotopographical polycaprolactone fibrous membrane (Zn 2+ @PT) via electrospinning to integrate immunomodulatory and osteogenic functions. In vitro studies demonstrated that the Zn 2+ @PT membrane effectively directs macrophage polarization toward the pro-regenerative M2 phenotype and enhances the osteogenic differentiation of bone marrow mesenchymal stem cells. In vivo results further revealed its ability to remodel the periodontitis immune microenvironment and boost alveolar bone regeneration. This work elucidates a synergistic mechanism between zinc ions and surface topography in promoting bone healing through a sequential regulatory logic, where early-stage immunomodulation paves the way for subsequent osteogenesis, providing a new material design strategy for sequentially regulated regeneration of inflammatory bone defects in periodontitis.

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Cite This Study

Zheng et al. (2026) studied this question.

synapsesocial.com/papers/69b256fe96eeacc4fcec5bcchttps://doi.org/10.1016/j.matdes.2026.115761
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