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April 1, 2026International Journal of Food Science & Technology0 citationsOpen Access

Characterization of bioactive compounds (GABA, glutathione, phenolic acids and isomaltooligosaccharides) and enhancement of GABA via mutagenesis during Shaoxing Huangjiu fermentation

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SZShufen ZhangJLJianghua LiJCJian Chen

Key Points

  • To characterize bioactive compounds during Shaoxing Huangjiu fermentation and enhance GABA production via mutagenesis.
  • Collected fermentation broth at Days 1, 5, 15, and 19 from batches with three replicates each.
  • Quantitative analysis measured levels of total polyphenols, GABA, glutathione, phenolic acids, and isomaltooligosaccharides.
  • Conducted GC-MS analysis to identify volatile bioactive compounds.
  • Applied gamma-ray mutagenesis to Saccharomyces cerevisiae N85 to create GABA-enhanced mutants.
  • Total polyphenols and GABA peaked on Day 15 at 576.83 mg/L and 215.12 mg/L, respectively.
  • Isomaltooligosaccharides peaked on Day 5 at 6.62 g/L.
  • The optimized mutant C59 showed a 72.09% increase in GABA yield compared to the wild type.

Abstract

Abstract Shaoxing Huangjiu contains bioactive compounds mediating its health benefits. To investigate these compounds during fermentation, 500 mL fermentation broth were collected at four time points (Days 1, 5, 15, and 19) with three biological replicates each. Quantitative analysis confirmed six target bioactive compounds. Total polyphenols, total flavonoids, and gamma-aminobutyric acid (GABA) remained above 100 mg/L throughout fermentation; total polyphenols and GABA reached maxima on Day 15 at 576.83±10.41 mg/L and 215.12±4.76 mg/L, respectively. Glutathione (GSH) and individual phenolic acids were below 4 mg/L. Isomaltooligosaccharides peaked on Day 5 at 6.62±1.73 g/L. GC-MS analysis identified nine potential volatile bioactive compounds (such as terpenoid alcohols and medium-chain fatty acids) at μg/L levels. This compositional shift was accompanied by microbial succession, with Saccharomyces cerevisiae becoming dominant (4.25% to 43.38%). Based on this, Saccharomyces cerevisiae N85 was subjected to 60Co gamma-ray mutagenesis to screen for GABA-enhanced mutants. The optimized mutant C59 exhibited a 72.09% increase in GABA yield. In this study, a traditional mutagenesis approach was employed to generate the GABA-enhanced mutant strain C59, offering a potential microbial candidate for future industrial application.

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Cite This Study

Zhang et al. (2026) studied this question.

synapsesocial.com/papers/69cd7a6f5652765b073a793chttps://doi.org/10.1093/ijfood/vvag063
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