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April 7, 2026Materials & Design0 citationsOpen Access

Structure–property–function relationships of supercritical CO2-processed amniotic membrane: An ex vivo ocular proof of concept

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LAL. AdamSRS. RotaFLFlora Lemaire

Key Points

  • The aim is to develop a sterile, readily available amniotic membrane using the modified Supercrit® process.
  • Used modified Supercrit® processing to alter amniotic membrane structure.
  • Compared the new membrane with traditional freeze-drying methods.
  • Conducted mechanical and biological property assessments.
  • Performed ex vivo ocular surface trials for handling and suturing.
  • m-Supercrit® processing produced a transparent and hydrophilic amniotic membrane.
  • Significant increase in the membrane’s linear elastic modulus was observed.
  • Reduction in bioactivity and cell migration, with lower levels of HGF and b-FGF.
  • The membrane retained essential biological functions such as cytocompatibility and anti-inflammatory properties.

Abstract

• Supercritical carbon dioxide alters amniotic membrane ultrastructure. • Correlations among elasticity, bioactivity, and matrix composition are demonstrated. • The scCO 2 process is a promising strategy for sterile off-the-shelf amniotic membrane. Human amniotic membrane (AM) exhibits a range of biological and structural properties that support its clinical use in regenerative medicine, particularly for ophthalmologic applications. This study aims to develop a readily available, sterile AM using modified (m)-Supercrit® process. Compared with freeze-drying, m-Supercrit® processing produces a transparent, thin, and hydrophilic membrane, key attributes for corneal applications. Mechanistically, m-Supercrit® processing induces marked alterations in collagen and glycosaminoglycan composition, which are associated with a significant increase in the membrane’s linear elastic modulus. Although m-Supercrit®-processed AM shows a reduction in bioactivity and cell migration, including a significant decrease in HGF and b-FGF levels, it retains essential biological functions such as hemocompatibility, cytocompatibility, cell adhesion/proliferation, anti-inflammatory, and anticancer activities. Importantly, the clinical feasibility of handling and suturing m-Supercrit®-processed AM is demonstrated in an ex vivo ocular surface model. Overall, these findings support the m-Supercrit® process as a promising strategy for developing an off-the-shelf, sterile amniotic membrane suitable for ophthalmologic clinical applications.

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Cite This Study

Adam et al. (2026) studied this question.

synapsesocial.com/papers/69d49f8ab33cc4c35a228085https://doi.org/10.1016/j.matdes.2026.115964
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