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April 29, 2026Organic & Biomolecular Chemistry0 citations

CSA-catalyzed three-component synthesis of 6-aryl-6 H -chromeno4,3- b quinolines

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MKM Dinesh KumarKYKomal YadavSSSatyajit Singh

Key Points

  • To develop an efficient method for synthesizing chromeno-quinoline derivatives using CSA-catalyzed reactions.
  • Three-component synthesis involving anilines, salicylaldehydes, and cinnamaldehydes.
  • Utilized (±)-camphorsulfonic acid as a catalyst.
  • Conducted reactions under mild conditions with gram-scale applicability.
  • Achieved significant atom economy compared to existing multistep approaches.
  • Demonstrated compatibility with various substrates, leading to precipitate formation.
  • Measured absolute quantum yield and studied aggregation behavior of chromeno-quinoline compounds.

Abstract

]quinoline derivatives from aromatic anilines, salicylaldehydes, and cinnamaldehydes under (±)-camphorsulfonic acid catalysis. The optimised protocol offers significant potential for atom economy under mild conditions over the pre-existing multistep approaches. This method is operationally simple and well compatible with a wide range of substrates, with most derivatives forming a precipitate in the reaction mixture. This new approach is followed to perform gram-scale synthesis, achieve smooth results, and demonstrate its industrial applicability. Moreover, chromeno-quinoline frameworks have demonstrated significant potential as pharmacophores and functional materials. The aggregation behaviour of one of the compounds, 4o, was also studied in a THF/hexane solvent, along with concentration-dependent fluorescence spectroscopy. Absolute quantum yield was also measured in both THF and hexane.

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Cite This Study

Kumar et al. (2026) studied this question.

synapsesocial.com/papers/69f154c0879cb923c4944f46https://doi.org/10.1039/d6ob00383d
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