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April 30, 2026Journal of Biological Chemistry0 citationsOpen Access

Platelet CLEC-2 activation leads to GPIb⍺ shedding: implications for doxorubicin chemotherapy and thrombosis

ZRZ. RousseauWMWenjing MaTLTianle Long

Key Result

Doxorubicin directly binds to platelet CLEC-2 with an affinity of 4.2 nM, leading to ADAM17-mediated shedding of GPIbα and reducing its surface expression by approximately 50% in human platelets.

Key Points

  • The study aims to explore the mechanism by which doxorubicin activates platelets and induces GPIb shedding.
  • Assessed platelet aggregation in response to Dox and other agonists in human and mouse models.
  • Utilized Isothermal Titration Calorimetry to measure Dox binding affinity to CLEC-2.
  • Investigated the role of specific inhibitors on GPIb shedding.
  • Dox inhibited CLEC-2 mediated platelet aggregation (4.2 nM binding affinity).
  • Significant GPIb shedding observed after Dox treatment, linked to ADAM17 activity.
  • Inhibition of ADAM10/17 reduced GPIb shedding, indicating a therapeutic target.

Structured PICO

Does doxorubicin induce GPIbα shedding via CLEC-2 activation in platelets?

P
Population
Human platelets from healthy volunteers, mouse platelets, C57BL/6 wild type mice, and αIIb-/- mice
I
Intervention
Doxorubicin and anti-CLEC-2 monoclonal antibody
C
Comparator
Vehicle control or isotype control
O
Outcome
Platelet aggregation, CLEC-2 binding affinity, and GPIbα sheddingsurrogate

Doxorubicin binds to platelet CLEC-2, leading to ADAM17-mediated GPIbα shedding, providing a mechanistic explanation for doxorubicin-induced platelet activation and thrombocytopenia.

Main Result

Absolute Event Rate: 50% vs 100%

Limitations

  • The disparity between prolonged in vitro and rapid in vivo GPIbα shedding suggests an uncharacterized dynamic element.
  • Cannot exclude contributions from intracellular granules or open canalicular system releasing glycocalicin.

Abstract

Doxorubicin (Dox) is a potent first-line chemotherapeutic and widely administered against different types of cancer, but is associated with a myriad of side effects, including cancer/chemotherapy-associated thrombosis and drug-induced thrombocytopenia (DIT).Although we and others have reported Dox-induced platelet activation, the binding partner of Dox on platelets has not been previously explored.Here, we found human and mouse platelet aggregation triggered via C-Type Lectin-like Receptor-2 (CLEC-2) was obstructed by Dox, but aggregation induced by classical agonists like ADP, collagen/collagen-related peptide, or thrombin receptoractivating peptide 6 (TRAP6), was unaffected.By Isothermal Titration Calorimetry, we detected a high binding affinity between Dox and recombinant CLEC-2 at 4.2 2.4 nM.Interestingly, we found significant GPIb shedding from human and mouse platelet surfaces following Dox treatment.Consistently, GPIb shedding was recapitulated following anti-CLEC-2 monoclonal antibody treatment.Using Piceatannol to selectively inhibit CLEC-2 intracellular signaling or the pan-Matrix Metalloproteinases (MMP) inhibitor GM6001 rescued GPIb from both Dox and CLEC-2 mAb-induced shedding.Using GI254023X or GW280264X to specifically inhibit ADAM10 or ADAMs10/17, respectively, revealed inhibition of ADAM10/17, but not ADAM10 exclusively, prohibited GPIb shedding.Collectively, this implicates the classical sheddase of GPIb, ADAM17.Thus, we pinpointed CLEC-2 as a binding partner for Dox on platelets and a novel pathway of ADAM17-mediated GPIb shedding via CLEC-2.These data not only provide insights into a mechanism of Dox-induced platelet activation, thrombosis, and DIT, but also reveal putative precision therapeutic approaches for Dox-treated patients and nominate CLEC-2 inhibition as a means to regulate thrombotic disease and/or bleeding disorders.

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Cite This Study

Rousseau et al. (2026) studied Healthy volunteers and murine models (preclinical). Doxorubicin vs. Vehicle control was evaluated on Surface GPIbα expression on human platelets. Doxorubicin directly binds to platelet CLEC-2 with an affinity of 4.2 nM, leading to ADAM17-mediated shedding of GPIbα and reducing its surface expression by approximately 50% in human platelets.

synapsesocial.com/papers/69f2f0991e5f7920c6386bfehttps://doi.org/10.1016/j.jbc.2026.113074
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