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May 9, 2026Minerals0 citationsOpen Access

The Selective Flotation Separation of Pyrite from Fine Chlorite and Sericite Using EDDS as a Novel Depressant

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YQYunlou QianYWYì WángXHXiaolong Huang

Key Points

  • This research aims to enhance the flotation separation of pyrite from fine chlorite and sericite using EDDS.
  • Conducted micro-flotation and mixed mineral flotation tests with EDDS as a depressant.
  • Performed zeta potential measurements and X-ray photoelectron spectroscopy (XPS) characterization to analyze interactions.
  • Optimized conditions at pH 8 and 200 mg/L EDDS to assess flotation performance.
  • EDDS reduced recoveries of sericite to ~20% and chlorite to ~15%, while pyrite recovery was restored to ~80%.
  • EDDS demonstrated strong chemical adsorption on sericite/chlorite, enhancing their hydrophilicity, while showing weak adsorption on pyrite.
  • At pH 8, over 90% of EDDS existed as HEDDS3−, enhancing selective adsorption on positively charged gangue.

Abstract

To solve the problem of mechanical entrainment and slime coating of fine sericite and chlorite hindering the flotation separation of gold-bearing pyrite in low-grade gold ores, ethylenediamine-N,N’-disuccinic acid (EDDS) was innovatively used as a selective and eco-friendly depressant. A systematic set of tests, including micro-flotation, artificial mixed mineral flotation, zeta potential measurement, adsorption capacity test, solution chemistry analysis and X-ray photoelectron spectroscopy (XPS) characterization, was conducted to explore its flotation performance and action mechanism. The results showed that pH 8 and 200 mg/L EDDS were the optimal conditions under which EDDS reduced the recoveries of sericite and chlorite to ~20% and ~15%, respectively, while restoring pyrite recovery to ~80% with a notable upgrade in concentrate grade. EDDS exhibited strong chemical adsorption on sericite and chlorite via chelating their active Al/Mg sites, significantly enhancing their hydrophilicity. In contrast, it only undergoes weak physical adsorption on pyrite, with negligible observed influence on its hydrophobicity and the adsorption of (sodium butyl xanthate) SBX. At pH 8, EDDS mainly existed as HEDDS3− (~90%), whose triple negative charge strengthened electrostatic interaction with positively charged gangue surfaces, boosting selective adsorption. This study confirms EDDS as a highly efficient depressant for pyrite–sericite/chlorite flotation under pure mineral and artificial mixed mineral conditions. Since the present study is based on pure minerals and artificial mixtures, further validation using real ore samples is still required before practical industrial application. This research expands the application of EDDS in mineral processing and provides a novel eco-friendly technical approach for the laboratory-scale separation of fine gold-bearing pyrite from low-grade gold ores with high clay gangue content.

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Cite This Study

Qian et al. (2026) studied this question.

synapsesocial.com/papers/69fed0abb9154b0b82877b52https://doi.org/10.3390/min16050489
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