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May 15, 2026Advances in Laboratory Medicine / Avances en Medicina de Laboratorio0 citationsOpen Access

Re-evaluating haemolysis rejection criteria for PT, aPTT, and D-dimer testing: evidence from paired clinical samples on the CN-3000 analyser

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JKJirapa KaewkhruawanWMWararat MasalaeSTSurapat Tanticharoenkarn

Key Points

  • The aim is to evaluate the impact of spontaneous haemolysis on coagulation assays and to analyze flagging behavior in haemolysed samples.
  • Analyzed 39 paired haemolysed (H) and non-haemolysed (NH) samples for PT, aPTT, and D-dimer on Sysmex CN-3000.
  • Compared mean biases to predefined critical differences derived from biological variation data.
  • Assessed analyser flagging with five sample pools across five haemolysis concentration levels.
  • Mean bias for PT was +0.07 s (p=0.5979), aPTT +0.44 s (p=0.8704), and D-dimer +0.72 mg/L FEU (p=0.0199).
  • D-dimer showed the highest relative bias but remained below critical difference (64.7%).
  • Haemolysis degree did not predict interference magnitude across analyzed hemoglobin concentrations.

Abstract

Abstract Objectives Haemolysis is the leading preanalytical cause of sample rejection in coagulation testing. This study prospectively evaluated the impact of spontaneous haemolysis on routine haemostasis assays by comparing paired haemolysed (H) and non-haemolysed (NH) clinical samples. Additionally, analyser flagging behaviour was characterised using an artificially haemolysed sample series. Methods Thirty nine paired of H and NH samples were analysed for prothrombin time (PT), activated partial thromboplastin time (aPTT), and D-dimer (DD) on the Sysmex CN-3000. Mean biases were compared against predefined critical differences (CD) derived from biological variation data. Analyser flagging was additionally assessed using five sample pools across five haemolysis concentration levels (H1–H5). Results When comparing H samples with NH samples, the mean bias was +0.07 s (+0.14 %) for PT (p=0.5979), +0.44 s (+0.66 %) for aPTT (p=0.8704), and +0.72 mg/L FEU (+10.63 %) for D-dimer (p=0.0199). D-dimer showed the highest relative bias but remained below the CD (64.7 %). Degree of haemolysis did not predict the magnitude of interference across the range of haemoglobin (Hb) concentrations studied. CN-3000 flagging grades were constant and correlated free Hb and irrespective of baseline sample PT/aPTT/D-dimer level. Conclusions Mild to moderate spontaneous haemolysis does not produce clinically significant interference in PT, aPTT, or D-dimer. CN-3000 flagging behaviour is predictable and grade-dependent. Re-evaluation of automatic haemolysis rejection thresholds is warranted.

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Cite This Study

Kaewkhruawan et al. (2026) studied this question.

synapsesocial.com/papers/6a06b9e2e7dec685947ac866https://doi.org/10.1515/almed-2026-0028
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