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May 17, 2026ACS Applied Materials & Interfaces0 citations

Molecular Structure Design of Dynamically Bonded Recyclable Commercial Polyurethane Foams for Enhanced Reprocessing Performance and Upcycling

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PWPeizhen WuXMXiaoping MoSLSihong Lin

Key Points

  • The central aim is to improve the recycling and reprocessing of commercial polyurethane foams by designing a novel cross-linker.
  • Utilized biosourced vanillin and 4,4'-dithiodianiline to create a dual dynamic bond cross-linker.
  • Conducted hot-pressing to facilitate exchange reactions with urethane bonds.
  • Assessed tensile strength and relaxation time for recycled materials.
  • Achieved a tensile strength of 81.50 MPa for recycled polyurethane plastic.
  • Demonstrated a short relaxation time of 15.6 seconds for excellent recyclability.
  • Produced a high-strength adhesive with a lap-shear strength of 16.34 MPa, lifting an 80 kg weight.

Abstract

Although commercial polyurethane foam (PUF) possessed significant recycling value, its permanently cross-linked structure made reprocessing and recycling highly challenging. This study utilized biosourced vanillin (VAN) and 4,4'-dithiodianiline (4-DTDA) to design a dual dynamic bond cross-linker (APDV) containing both S-S bonds and C═N bonds for the recycling and reprocessing of commercial PUF. Under hot-pressing conditions, the hydroxyl groups in APDV underwent exchange reactions with the urethane bonds in the polyurethane chains, enabling the one-step conversion of commercial PUF into high-performance plastics and adhesives. The recycled polyurethane plastic achieved a tensile strength of up to 81.50 MPa, while the presence of dual dynamic bonds resulted in a short relaxation time (τ = 15.6 s), endowing the material with excellent recyclability for multiple reuse cycles. Furthermore, the commercial PUF can be transformed into a high-strength adhesive with a lap-shear strength of 16.34 MPa, which was capable of easily lifting an 80 kg adult. This study provided a sustainable and implementable strategy for the recycling and reprocessing of commercial PUF.

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Cite This Study

Wu et al. (2026) studied this question.

synapsesocial.com/papers/6a095af37880e6d24efe0af0https://doi.org/10.1021/acsami.6c02877
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