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May 20, 2026Journal of the American Chemical Society0 citations

Kinetic Scaling Rules Governing Phase Instability in Perovskite Halides

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BBBiswajit BallECEthan R. CronkWXWenjun Xiang

Key Points

  • The study aims to understand the mechanisms behind phase instability in perovskite halides, focusing on ion-migration kinetics.
  • Conducted first-principles calculations alongside experimental validations
  • Identified scaling relationships linking instability temperatures to ion-migration barriers
  • Analyzed both single and double perovskite chemistries
  • Decomposition temperature increases linearly with the resistance of A–X and B–X migration barriers (exact metrics not provided)
  • Cubic-to-tetragonal transition temperature is determined by the differential shift in migration barriers along the c-axis
  • Proposed a general design principle for creating stable halide perovskites

Abstract

Perovskite halides (ABX3) offer remarkable promise for next-generation electronic and optoelectronic technologies, yet their deployment is fundamentally limited by intrinsic thermal phase instability. Despite extensive study, the mechanisms governing decomposition and structural transitions remain unresolved, partly because prevailing stability metrics emphasize thermodynamics while overlooking the coupled ion-migration kinetics that dominate degradation. Here, we identify two universal linear scaling relationships that quantitatively link macroscopic instability temperatures to microscopic ion-migration kinetics. Using first-principles calculations combined with experimental validations across diverse single and double perovskite chemistries, we show that the decomposition temperature of cubic perovskite halides increases linearly with the composite serial “resistance” of A–X and B–X migration barriers, capturing the coupled kinetic difficulty of bond rupture required for lattice breakdown. In contrast, the cubic-to-tetragonal transition temperature scales with a distinct kinetic descriptor: the differential shift in cation and anion migration barriers projected along the crystallographic c-axis, which governs the ease of symmetry-breaking distortions. Together, these relationships enable accurate prediction of instability temperatures across a broad chemical space and reconcile previously disparate observations of perovskite stability. By revealing composite ion-migration kinetics as the dominant unifying driver of phase instability, this work provides a general design principle for engineering intrinsically stable halide perovskites and overcoming a central bottleneck in their technological maturation.

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Cite This Study

Ball et al. (2026) studied this question.

synapsesocial.com/papers/6a0d5098f03e14405aa9c7c2https://doi.org/10.1021/jacs.6c01689
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