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May 20, 2026Luminescence0 citations

Luminescence of N 2 ,3‐etheno‐2‐aminopurine Embedded in Polyvinyl Alcohol Films at Room Temperature

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BWBeata Wielgus‐KutrowskaJWJacek WierzchowskiASAlicja Stachelska‐Wierzchowska

Key Points

  • This research aims to investigate the luminescence characteristics of N2,3‐etheno‐2‐aminopurine embedded in polyvinyl alcohol films.
  • Used steady-state and time-resolved spectroscopy to analyze luminescence properties.
  • Embedded N2,3‐ε2APu in poly(vinyl alcohol) to assess fluorescence and phosphorescence.
  • Examined the effects of UV excitation and lifetime distribution in the polymer matrix.
  • N2,3‐ε2APu shows a central fluorescence lifetime of about 5 ns with a Lorentzian distribution half-width of 2 ns.
  • The films demonstrate strong room-temperature phosphorescence peaking at 500 nm with a lifespan of approximately 0.15 s.
  • Excitation at wavelengths above 400 nm results in high positive phosphorescence anisotropy of 0.3.

Abstract

ABSTRACT The luminescence properties of N 2 ,3‐etheno‐2‐aminopurine (N 2 ,3‐ε2APu) have been studied using steady‐state and time‐resolved spectroscopy. N 2 ,3‐ε2APu was embedded in poly(vinyl alcohol) (PVA) polymer, which is known for effective immobilization of dissolved fluorophore molecules. Upon UV excitation, N 2 ,3‐ε2APu shows a bright dark‐blue fluorescence with high fluorescence anisotropy, indicating efficient immobilization. Time‐resolved fluorescence measurements show a somewhat heterogeneous lifetime, requiring a lifetime distribution model to fit the data. The fit reveals a central lifetime of about 5 ns and a half‐width of the Lorentzian distribution of about 2 ns. We attribute this lifetime spread to the varying surroundings of fluorophore molecules in the polymer matrix. The N 2 ,3‐ε2APu‐doped PVA films exhibit strong room‐temperature phosphorescence (RTP) centered at 500 nm, with a lifetime of approximately 0.15 s. The excitation at 330 nm results in negative phosphorescence anisotropy. Interestingly, N 2 ,3‐ε2APu–doped PVA films can be directly excited to a triplet state at longer wavelengths (above 400 nm). This excitation results in a high positive phosphorescence anisotropy, reaching a value of 0.3 at about 450 nm. The ability to excite a molecule at longer wavelengths may find applications in the biomedical sciences, particularly in the study of photo‐chemically labile proteins and their complexes with emitting ligands.

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Cite This Study

Wielgus‐Kutrowska et al. (2026) studied this question.

synapsesocial.com/papers/6a0d50aff03e14405aa9cac6https://doi.org/10.1002/bio.70495
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