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May 27, 2026ChemistrySelect0 citations

A Concise Thermal Synthesis of Nitrogen Doped Mesoporous Carbon/Ti 3 C 2 Nanocomposite Modified Electrode for Sensitive Detection of Isoquercetin

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WLWei LiuNWNannan WangZDZhangyu Dai

Key Points

  • This research aims to develop a nitrogen-doped mesoporous carbon/Ti3C2 nanocomposite electrode for the sensitive detection of isoquercetin.
  • Utilized a simple thermal synthesis method to create nitrogen-doped mesoporous carbon spheres.
  • Characterized the nanocomposite using SEM, EDS, XPS, FTIR, and electrochemical methods.
  • Evaluated the performance of the modified glassy carbon electrode for isoquercetin detection.
  • Achieved a wide linear detection range of 0.1–100 µM for isoquercetin.
  • Established a low detection limit of 0.073 µM (S/N = 3) for the modified electrode.
  • Demonstrated good selectivity and excellent anti-interference performance in actual sample detection.

Abstract

ABSTRACT This article is based on Zn‐MOF‐8 and uses a simple thermal synthesis method to prepare nitrogen‐doped mesoporous carbon spheres (NMC), which is then combined with Ti 3 C 2 to prepare NMC/Ti 3 C 2 nanocomposites. It was characterized by SEM, EDS, XPS, FTIR, and electrochemical methods. The NMC/Ti 3 C 2 nanocomposite modified glassy carbon electrode (GCE) was used for sensitive detection of isoquercetin (IQ), achieving a wide linear range of 0.1–100 µM and a low detection limit of 0.073 µM (S/N = 3). The modified electrode also exhibits good selectivity, excellent anti‐interference performance and can be used for actual sample detection.

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Cite This Study

Liu et al. (2026) studied this question.

synapsesocial.com/papers/6a168b160c924ddd1bd59f52https://doi.org/10.1002/slct.73535
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