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May 28, 2026Powder Metallurgy0 citationsOpen Access

Tailoring microstructure and properties of Ti-6Al-4V from piston-based material extrusion through hot isostatic pressing

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KBKatharina BartschDHDirk HerzogLWLennart Waalkes

Key Points

  • This research aims to investigate how microstructure and mechanical properties of Ti-6Al-4V can be optimized using PEX and HIP processes.
  • Utilized piston-based material extrusion (PEX) to create green parts from Ti-6Al-4V feedstock.
  • Applied hot isostatic pressing (HIP) under both standard and high-purity conditions to enhance microstructure and properties.
  • Evaluated changes in density, microstructure, and mechanical properties post-HIP.
  • Mean density of sintered parts reached 97.2%; post-HIP density increased to 98.9–99.3%.
  • Using Quintus Purus® HIP resulted in increased yield and ultimate tensile strength with minimal reduction in elongation.
  • Standard HIP showed a similar trend but with slightly greater effect on mechanical properties.

Abstract

Piston-based material extrusion (PEX) is an additive manufacturing technology that enables the processing of metal injection moulding (MIM) feedstock to form green parts. The extrusion process does not require moulds and hence is a competitive alternative for the shaping of MIM process routes, offering short lead times and cost-efficiency for lower lot sizes, while integrating into the remaining process chain and equipment. This paper focuses on the microstructure and properties of Ti-6Al-4V fabricated by PEX and followed by a subsequent hot isostatic pressing (HIP) step for parts requiring superior density and mechanical properties. The HIP process is performed using standard as well as high-purity conditions (Quintus Purus ® ). After sintering, a globular, mostly α microstructure is observed. A subsequent HIP followed by rapid quenching transforms the microstructure to a bi-modal state. A similar effect on microstructure is observed for the Quintus Purus ® HIP; however, the formation of α-case on the part surface is avoided. While the mean density of the sintered parts is 97.2%, HIP leads to an increase to 98.9–99.3% with the remnant porosity mainly stemming from open, connected pores. Although the sintered specimens already fulfil the industrial requirements, the Quintus Purus ® HIP leads to a slight increase in yield and ultimate tensile strength at minimal reduction of elongation. The standard HIP shows the same but slightly more pronounced trend. The results show that by a careful design of the specific HIP conditions, the microstructure and properties can be tailored for a specific application.

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Cite This Study

Bartsch et al. (2026) studied this question.

synapsesocial.com/papers/6a17dcbb3fad632b0f9d9724https://doi.org/10.1177/00325899261454936
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